GC-MS Characterisation of Sapogenins from Sisal Waste and a Method to Isolate Pure Hecogenin

نویسندگان

  • Jener David G. Santos
  • Alexsandro Branco
چکیده

Five steroidal sapogenins (tigogenin, neotigogenina, hecogenin, gloriogenin, and dehydrohecogenin) were characterised by gas chromatography coupled with mass spectrometry (GC-MS) from a hydrolysed extract of sisal waste. In addition, pure hecogenin, an important raw material for the pharmaceutical industry, was obtained from this waste by selective liquid-liquid extraction of saponins with only hecogenin as aglycone, followed by acid hydrolysis. The yield of pure hecogenin was 460 mg.Kg -1 of sisal waste.

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تاریخ انتشار 2014